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Evolution of dispersion of carbon nanotubes in Polyamide 11 matrix composites as determined by DC conductivity

Carponcin, Delphine and Dantras, Eric and Aridon, Gwenaëlle and Levallois, Franck and Cadiergues, Laurent and Lacabanne, Colette Evolution of dispersion of carbon nanotubes in Polyamide 11 matrix composites as determined by DC conductivity. (2012) Composites Science and Technology, 72 (4). 515-520. ISSN 0266-3538

(Document in English)

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Official URL: http://dx.doi.org/10.1016/j.compscitech.2011.12.012


Double-walled Carbon NanoTubes (DWCNTs) have been dispersed in a Polyamide 11 (PA11) matrix by two routes: in the solvent way, Polyamide 11 was first dissolved in its solvent to ensure a liquid state dispersion of carbon nanotubes by ultrasonic way; in the melt mixing way, an optimization of the extrusion parameters, such as mixing time, mixing speed, mixing temperature and screw rotation direction allow to reach satisfactory dispersion. Dispersion and percolation threshold have been compared thanks to the evolution of DC conductivity with carbon nanotubes weight fraction in Polyamide 11. An electrical percolation threshold of 1% in weight was found by the solvent way while the melt mixing way offers one of the lower percolation thresholds for a semi-crystalline matrix (0.93% in weight). An interpretation of the limitation of the electrical percolation threshold value in a semi-crystalline matrix will be proposed.

Item Type:Article
Additional Information:Thanks to Elsevier editor. The original version is available at http://www.sciencedirect.com The original PDF of the article can be found at http://www.sciencedirect.com/science/article/pii/S0266353811004477
HAL Id:hal-03531123
Audience (journal):International peer-reviewed journal
Uncontrolled Keywords:
Institution:French research institutions > Centre National d'Études Spatiales - CNES (FRANCE)
French research institutions > Centre National de la Recherche Scientifique - CNRS (FRANCE)
Other partners > EADS - Astrium (FRANCE)
Université de Toulouse > Institut National Polytechnique de Toulouse - Toulouse INP (FRANCE)
Université de Toulouse > Université Toulouse III - Paul Sabatier - UT3 (FRANCE)
Laboratory name:
Deposited On:04 May 2012 13:07

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