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Sugarcane bagasse mild alkaline fractionation and production of purified fractions by pulse chromatography with water

Oriez, Vincent and Beyerle, Marlène and Pontalier, Pierre-Yves and Peydecastaing, Jérôme Sugarcane bagasse mild alkaline fractionation and production of purified fractions by pulse chromatography with water. (2018) Industrial Crops and Products, 125. 370-378. ISSN 0926-6690

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Official URL: https://doi.org/10.1016/j.indcrop.2018.09.019

Abstract

Sugarcane bagasse (SCB) was treated under mild alkaline conditions (solid:liquid ratio of 1:20 (w/v), 1.5% NaOH (w/v), 60 °C, 6 h) to fractionate the lignocellulose in order to produce a typical mild alkaline extract from a lignocellulosic biomass. The solid residue was enriched in cellulose, while the SCB alkaline extract contained lignin and hemicelluloses, but also inorganic salts, five phenolic monomers and acetic acid. After concentration of the alkaline extract by evaporation, low pressure chromatography with water as eluent was performed to produce purified fractions. Two different strong acid cation (SAC) exchange resins were tested: one gel-type resin and one macroporous-type resin. The lignin and hemicelluloses were separated from the inorganic salts by the gel-type SAC exchange resin. On this resin, the phenolic monomers were partitioned regarding the presence or absence in their structure of a carboxyl group. On the macroporous-type SAC exchange resin, the largest sugar oligomers and lignin oligomers were obtained in a fraction free of inorganic salts, phenolic monomers and acetic acid.

Item Type:Article
HAL Id:hal-02369701
Audience (journal):International peer-reviewed journal
Uncontrolled Keywords:
Institution:Université de Toulouse > Institut National Polytechnique de Toulouse - Toulouse INP (FRANCE)
French research institutions > Institut National de la Recherche Agronomique - INRA (FRANCE)
Other partners > Novasep (FRANCE)
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Funders:
Agence Nationale de la Recherche - ANR
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Deposited On:19 Nov 2019 09:13

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