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Full elastic strain tensor determination at the phase scale in a powder metallurgy nickel-based superalloy using X-ray Laue microdiffraction

Altinkurt, Gader and Fèvre, Mathieu and Robach, Odile and Micha, Jean-Sébastien and Geandier, Guillaume and Dehmas, Moukrane Full elastic strain tensor determination at the phase scale in a powder metallurgy nickel-based superalloy using X-ray Laue microdiffraction. (2017) Journal of Applied Crystallography, 50 (6). 1754-1765. ISSN 0021-8898

(Document in English)

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Official URL: http://dx.doi.org/10.1107/S1600576717014558


Laue microdiffraction is used to determine the full elastic strain tensor of the γ and γ′ phases in grains of a nickel-based superalloy with a coarse-grained microstructure. A `rainbow' filter and an energy dispersive point detector are employed to measure the energy of Bragg reflections. For the two techniques, an uncertainty of ±2.5 × 10−3 Å is obtained for the undetermined crystal lattice parameter. Our measurements show that the filter method provides better confidence, energy resolution, accuracy and acquisition time. The sensitivity of each method with respect to the γ–γ′ lattice mismatch is demonstrated with measurements in samples with average precipitate sizes of 200 and 2000 nm. For the 200 nm precipitate size, the lattice mismatch is less than 2 × 10−3 Å and the dilatational strains are close to ±1.5 × 10−3 depending on the considered phase. For the 2000 nm precipitate size, the lattice mismatch is close to 8 × 10−3 Å and almost no elastic strain occurs in the microstructure.

Item Type:Article
Additional Information:Thanks to International Union of Crystallography editor. The original PDF of the article can be found at Journal of Applied Crystallography website : http://scripts.iucr.org/cgi-bin/paper?S1600576717014558http://www.sciencedirect.com/science/journal/00406031
Audience (journal):International peer-reviewed journal
Uncontrolled Keywords:
Institution:French research institutions > Commissariat à l'Energie Atomique et aux énergies alternatives - CEA (FRANCE)
French research institutions > Centre National de la Recherche Scientifique - CNRS (FRANCE)
Université de Toulouse > Institut National Polytechnique de Toulouse - Toulouse INP (FRANCE)
French research institutions > Office National d'Etudes et Recherches Aérospatiales - ONERA (FRANCE)
Other partners > Université Grenoble Alpes - UGA (FRANCE)
Université de Toulouse > Université Toulouse III - Paul Sabatier - UT3 (FRANCE)
Other partners > Université de Lorraine (FRANCE)
Laboratory name:
Deposited On:20 Dec 2017 17:14

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