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Experimental investigation on the effect of nanostructuration on the adherence properties of epoxy adhesives by a probe tack test

Tramis, Olivier and Brethous, Romain and Hassoune-Rhabbour, Bouchra and Fazzini, Marina and Nassiet, Valérie Experimental investigation on the effect of nanostructuration on the adherence properties of epoxy adhesives by a probe tack test. (2015) International Journal of Adhesion & Adhesives, 67. 22-30. ISSN 0143-7496

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Official URL: http://dx.doi.org/10.1016/j.ijadhadh.2015.12.021

Abstract

In this work, we aimed to characterize the energy of adherence of nanoscale structured epoxy adhesives Diglycidyl ether of bisphenol-A/Methylene–diethylaniline(DGEBA/MDEA)induced by phase separation triblock copolymers Poly(MethacrylatedeMethyl)-b-Poly(ButylAcrylate)-b-Poly(MethylMethacrylate) (PMMA-b-PBA-b-PMMA) at gel state by a probe tack test,which is an original use of this kind of test for thermoset adhesives. For a set of mechanical parameters(probe’s roughness,contacttime,contact pressure and debonding velocity),we measured the energy of adherence for both neat and filled adhesives. The probe tack test was performed at different steps of gelation. We compared the behavior of the adhesives and evaluated the dissipation contribution to the energy of adherence of the adhesives during the test. We finally discussed the nanoparticles'influence on the competition between cavitation and fibrillation. We report that the addition of nanoparticles leads to an overall improvement of the energy of adherence, with a significant increase of the dissipation contribution to the energy measured.

Item Type:Article
Additional Information:Thanks to Elsevier editor. The definitive version is available at : http://www.sciencedirect.com/journal/international-journal-of-adhesion-and-adhesives
HAL Id:hal-01657900
Audience (journal):International peer-reviewed journal
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Institution:Université de Toulouse > Institut National Polytechnique de Toulouse - Toulouse INP (FRANCE)
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Deposited On:14 Nov 2017 10:18

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