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Scalable synthesis of ionic liquids: comparison of performances of microstructured and stirred batch reactors

Iken, Hicham and Guillen, Frédéric and Chaumat, Hélène and Mazières, Marie-Rose and Plaquevent, Jean-Christophe and Tzedakis, Theodore Scalable synthesis of ionic liquids: comparison of performances of microstructured and stirred batch reactors. (2012) Tetrahedron, vol. 53 (n° 27). pp. 3474-3477. ISSN 0040-4039

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Official URL: http://dx.doi.org/10.1016/J.TETLET.2012.04.119

Abstract

A range of alkylpyridinium bromide ionic liquids have been synthesized in a stirred reactor at multigram scale and characterized by physical methods (viscosity, conductivity, melting point, electrochemical window, and water content). One ionic liquid, octylpyridinium bromide, was chosen to be synthesized in both macro and reduced scale reactors, in order to compare its performance and to afford evidence of the advantages of a cross channel micro reactor (channel width = 1 mm) compared to a stirred reactor.

Item Type:Article
Additional Information:Thanks to Elsevier editor. The definitive version is available at http://www.sciencedirect.com The original PDF of the article can be found at : http://www.sciencedirect.com/science/article/pii/S0040403912007253
Audience (journal):International peer-reviewed journal
Uncontrolled Keywords:
Institution:French research institutions > Centre National de la Recherche Scientifique - CNRS
Université de Toulouse > Institut National Polytechnique de Toulouse - INPT
Université de Toulouse > Université Paul Sabatier-Toulouse III - UPS
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Deposited By:Audrey LEFEVRE

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